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ASTM D1157

ASTM D1157 – Standard Test Method for Total Inhibitor Content (TBC) of Light Hydrocarbons

Description:

Significance and Use

4.1 p-tertiary-butylcatechol is commonly added to commercial butadiene in amounts of 50 mg/kg to 250 mg/kg as an oxidation inhibitor. This test method is suitable for use by both producers and users of butadiene within the limitations described in Section 1.

Scope

1.1 This test method covers the determination of total p-tertiary-butylcatechol inhibitor added to polymerization and recycle grades of butadiene or to other C4 hydrocarbon mixtures containing no phenolic material other than catechol or no oxidized phenolic material other than that derived from oxidation of catechol. In general, all phenols and their quinone oxidation products are included in the calculated catechol content. Small amounts of polymer do not interfere. This test method is applicable over the range of TBC from 50 mg/kg to 500 mg/kg.

1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

Related Test Methods

ASTM D4865

ASTM D4860

ASTM D4857

ASTM D4850

ASTM D4839

ASTM D4833

ASTM D483

ASTM D4829

ASTM D4828

ASTM D4824

ASTM D482

ASTM D4815

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