ASTM D1747 – Standard Test Method for Refractive Index of Viscous Materials
Description:
Significance and Use
5.1 Refractive index is a fundamental physical property that can be used in conjunction with other properties to characterize pure hydrocarbons and their mixtures.
5.2 The use of refractive index in correlative methods for the determination of the gross composition of viscous oils and waxes often requires its measurement at elevated temperatures.
Scope
1.1 This test method covers the measurement of refractive indexes, accurate to two units in the fourth decimal place, of transparent and light-colored viscous hydrocarbon liquids and melted solids that have refractive indexes in the range between 1.33 and 1.60, and at temperatures from 80 °C to 100 °C. Temperatures lower than 80 °C can be used provided that the melting point of the sample is at least 10 °C below the test temperature.
1.2 This test method is not applicable, within the accuracy stated, to liquids having colors darker than ASTM Color No. 4, ASTM color as determined by Test Method D1500, to liquids which smoke or vaporize readily at the test temperature, or to solids melting within 10 °C of the test temperature.
NOTE 1: The instrument can be successfully used for refractive indices above 1.60; but since certified liquid standards for ranges above 1.60 are not yet available, the accuracy of measurement under these conditions has not been evaluated.
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.4 Warning—Mercury has been designated by EPA and many state agencies as a hazardous material that can cause central nervous system, kidney, and liver damage. Mercury, or its vapor, may be hazardous to health and corrosive to materials. Caution should be taken when handling mercury and mercury-containing products. See the applicable product Material Safety Data Sheet (MSDS) for details and EPA’s website (http://www.epa.gov/mercury/faq.htm) for additional information. Users should be aware that selling mercury or mercury-containing products, or both, in your state may be prohibited by state law.
ASTM D1744