ASTM D256 – Standard Test Methods for Determining the Izod Pendulum Impact Resistance of Plastics
Significance and Use
5.1 Before proceeding with these test methods, reference should be made to the specification of the material being tested. Any test specimen preparation, conditioning, dimensions, and testing parameters covered in the materials specification shall take precedence over those mentioned in these test methods. If there is no material specification, then the default conditions apply.
5.2 The pendulum impact test indicates the energy to break standard test specimens of specified size under stipulated parameters of specimen mounting, notching, and pendulum velocity-at-impact.
5.3 The energy lost by the pendulum during the breakage of the specimen is the sum of the following:
5.3.1 Energy to initiate fracture of the specimen;
5.3.2 Energy to propagate the fracture across the specimen;
5.3.3 Energy to throw the free end (or ends) of the broken specimen (“toss correction”);
5.3.4 Energy to bend the specimen;
5.3.5 Energy to produce vibration in the pendulum arm;
5.3.6 Energy to produce vibration or horizontal movement of the machine frame or base;
5.3.7 Energy to overcome friction in the pendulum bearing and in the indicating mechanism, and to overcome windage (pendulum air drag);
5.3.8 Energy to indent or deform plastically the specimen at the line of impact; and
5.3.9 Energy to overcome the friction caused by the rubbing of the striker (or other part of the pendulum) over the face of the bent specimen.
5.4 For relatively brittle materials, for which fracture propagation energy is small in comparison with the fracture initiation energy, the indicated impact energy absorbed is, for all practical purposes, the sum of factors 5.3.1 and 5.3.3. The toss correction (see 5.3.3) may represent a very large fraction of the total energy absorbed when testing relatively dense and brittle materials. Test Method C shall be used for materials that have an Izod impact resistance of less than 27 J/m (0.5 ft·lbf/in.). (See Appendix X4 for optional units.) The toss correction obtained in Test Method C is only an approximation of the toss error, since the rotational and rectilinear velocities may not be the same during the re-toss of the specimen as for the original toss, and because stored stresses in the specimen may have been released as kinetic energy during the specimen fracture.
5.5 For tough, ductile, fiber filled, or cloth-laminated materials, the fracture propagation energy (see 5.3.2) may be large compared to the fracture initiation energy (see 5.3.1). When testing these materials, factors (see 5.3.2, 5.3.5, and 5.3.9) can become quite significant, even when the specimen is accurately machined and positioned and the machine is in good condition with adequate capacity. (See Note 7.) Bending (see 5.3.4) and indentation losses (see 5.3.8) may be appreciable when testing soft materials.
NOTE 7: Although the frame and base of the machine should be sufficiently rigid and massive to handle the energies of tough specimens without motion or excessive vibration, the design must ensure that the center of percussion be at the center of strike. Locating the striker precisely at the center of percussion reduces vibration of the pendulum arm when used with brittle specimens. However, some losses due to pendulum arm vibration, the amount varying with the design of the pendulum, will occur with tough specimens, even when the striker is properly positioned.
5.6 In a well-designed machine of sufficient rigidity and mass, the losses due to factors 5.3.6 and 5.3.7 should be very small. Vibrational losses (see 5.3.6) can be quite large when wide specimens of tough materials are tested in machines of insufficient mass, not securely fastened to a heavy base.
5.7 With some materials, a critical width of specimen may be found below which specimens will appear ductile, as evidenced by considerable drawing or necking down in the region behind the notch and by a relatively high-energy absorption, and above which they will appear brittle as evidenced by little or no drawing down or necking and by a relatively low-energy absorption. Since these methods permit a variation in the width of the specimens, and since the width dictates, for many materials, whether a brittle, low-energy break or a ductile, high energy break will occur, it is necessary that the width be stated in the specification covering that material and that the width be reported along with the impact resistance. In view of the preceding, one should not make comparisons between data from specimens having widths that differ by more than a few mils.
5.8 The type of failure for each specimen shall be recorded as one of the four categories listed as follows:
|C =||Complete Break—A break where the specimen separates into two or more pieces.|
|H =||Hinge Break—An incomplete break, such that one part of the specimen cannot support itself above the horizontal when the other part is held vertically (less than 90° included angle).|
|P =||Partial Break—An incomplete break that does not meet the definition for a hinge break but has fractured at least 90 % of the distance between the vertex of the notch and the opposite side.|
|NB =||Non-Break—An incomplete break where the fracture extends less than 90 % of the distance between the vertex of the notch and the opposite side.|
For tough materials, the pendulum may not have the energy necessary to complete the breaking of the extreme fibers and toss the broken piece or pieces. Results obtained from “non-break” specimens shall be considered a departure from standard and shall not be reported as a standard result. Impact resistance cannot be directly compared for any two materials that experience different types of failure as defined in the test method by this code. Averages reported must likewise be derived from specimens contained within a single failure category. This letter code shall suffix the reported impact identifying the types of failure associated with the reported value. If more than one type of failure is observed for a sample material, then the report will indicate the average impact resistance for each type of failure, followed by the percent of the specimens failing in that manner and suffixed by the letter code.
5.9 The value of the impact methods lies mainly in the areas of quality control and materials specification. If two groups of specimens of supposedly the same material show significantly different energy absorptions, types of breaks, critical widths, or critical temperatures, it may be assumed that they were made of different materials or were exposed to different processing or conditioning environments. The fact that a material shows twice the energy absorption of another under these conditions of test does not indicate that this same relationship will exist under another set of test conditions. The order of toughness may even be reversed under different testing conditions.
NOTE 8: A documented discrepancy exists between manual and digital impact testers, primarily with thermoset materials, including phenolics, having an impact value of less than 54 J/m (1 ft-lb/in.). Comparing data on the same material, tested on both manual and digital impact testers, may show the data from the digital tester to be significantly lower than data from a manual tester. In such cases a correlation study may be necessary to properly define the true relationship between the instruments.
1.1 These test methods cover the determination of the resistance of plastics to “standardized” (see Note 1) pendulum-type hammers, mounted in “standardized” machines, in breaking standard specimens with one pendulum swing (see Note 2). The standard tests for these test methods require specimens made with a milled notch (see Note 3). In Test Methods A, C, and D, the notch produces a stress concentration that increases the probability of a brittle, rather than a ductile, fracture. In Test Method E, the impact resistance is obtained by reversing the notched specimen 180° in the clamping vise. The results of all test methods are reported in terms of energy absorbed per unit of specimen width or per unit of cross-sectional area under the notch. (See Note 4.)
NOTE 1: The machines with their pendulum-type hammers have been “standardized” in that they must comply with certain requirements, including a fixed height of hammer fall that results in a substantially fixed velocity of the hammer at the moment of impact. However, hammers of different initial energies (produced by varying their effective weights) are recommended for use with specimens of different impact resistance. Moreover, manufacturers of the equipment are permitted to use different lengths and constructions of pendulums with possible differences in pendulum rigidities resulting. (See Section 5.) Be aware that other differences in machine design may exist. The specimens are “standardized” in that they are required to have one fixed length, one fixed depth, and one particular design of milled notch. The width of the specimens is permitted to vary between limits.
NOTE 2: Results generated using pendulums that utilize a load cell to record the impact force and thus impact energy, may not be equivalent to results that are generated using manually or digitally encoded testers that measure the energy remaining in the pendulum after impact.
NOTE 3: The notch in the Izod specimen serves to concentrate the stress, minimize plastic deformation, and direct the fracture to the part of the specimen behind the notch. Scatter in energy-to-break is thus reduced. However, because of differences in the elastic and viscoelastic properties of plastics, response to a given notch varies among materials. A measure of a plastic’s “notch sensitivity” may be obtained with Test Method D by comparing the energies to break specimens having different radii at the base of the notch.
NOTE 4: Caution must be exercised in interpreting the results of these standard test methods. The following testing parameters may affect test results significantly:
|Method of fabrication, including but not limited to processing|
|technology, molding conditions, mold design, and thermal|
|Method of notching;|
|Speed of notching tool;|
|Design of notching apparatus;|
|Quality of the notch;|
|Time between notching and test;|
|Test specimen thickness,|
|Test specimen width under notch, and|
1.2 The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only.