ASTM D3798

ASTM D3798 – ASTM D3798 – Standard Test Method for Analysis of p-Xylene by Gas Chromatography (Withdrawn 2009)

Description:

Significance and Use

This test method is suitable for setting specifications on p-xylene and for use as an internal quality control tool where p-xylene is produced or is used in a manufacturing process. It may also be used in development or research work involving p-xylene. It is generally applied to determining those commonly occurring impurities such as nonaromatic hydrocarbons, benzene, toluene, ethylbenzene, m-xylene, o-xylene, and cumene (isopropylbenzene).

Purity is commonly reported by subtracting the determined expected impurities from 100.00. However, a gas chromatographic analysis cannot determine absolute purity if unknown components are contained within the material being examined. Refer to Specification D 5136 for determining other chemical and physical properties of p-xylene.

Scope

1.1 This test method covers the determination of known hydrocarbon impurities in, and the purity of p-xylene by gas chromatography (GC). It is generally meant for the analysis of p-xylene of 99 % or greater purity. Impurity concentrations that can be measured range from 0.001 to 1.000 weight %.

1.2 The following applies to all specified limits in this test method: for purposes of determining conformance with this test method, an observed value or a calculated value shall be rounded off ‘to the nearest unit’ in the right-hand digit used in expressing the specification limit, in accordance with the rounding-off method of Practice E 29