• Skip to main content
  • Skip to header right navigation
  • Skip to site footer

1-800-685-2088 | support@mat-cs.com

  • LinkedIn
MAT-CS - Materials Characterization Services

Materials Characterization Services

  • Home
  • About
    • Meet the Team
    • Consulting
  • Analytical Techniques
    • Bulk Analysis
    • Microscopy and Microanalytical
    • Surface and Thin Film
    • Polymer Characterization
    • Optical Measurements
    • Liquids and Gases
    • Electrical / Electronics
    • Reliability Testing
    • Miscellaneous
  • Test Methods
    • ASTM Methods List
    • ISO Methods List
    • AATCC
    • AOAC
    • AOCS
    • EPA, SM
    • FDA BAM
    • IP
    • JEDEC
    • MIL-STD
    • OCSPP
    • OPPTS
    • REACH
    • RoHS
    • SEMI
    • TAPPI
    • USP/EP/JP
  • Resources
    • Experiment Design
    • Consulting
    • The Laboratory Landscape
    • Quality Programs
    • Regulatory-Based Analyses
  • Contact
  • Get a Quote!
  • Home
  • About
    • Meet the Team
    • Consulting
  • Analytical Techniques
    • Bulk Analysis
    • Microscopy and Microanalytical
    • Surface and Thin Film
    • Polymer Characterization
    • Optical Measurements
    • Liquids and Gases
    • Electrical / Electronics
    • Reliability Testing
    • Miscellaneous
  • Test Methods
    • ASTM Methods List
    • ISO Methods List
    • AATCC
    • AOAC
    • AOCS
    • EPA, SM
    • FDA BAM
    • IP
    • JEDEC
    • MIL-STD
    • OCSPP
    • OPPTS
    • REACH
    • RoHS
    • SEMI
    • TAPPI
    • USP/EP/JP
  • Resources
    • Experiment Design
    • Consulting
    • The Laboratory Landscape
    • Quality Programs
    • Regulatory-Based Analyses
  • Contact
  • Get a Quote!
MAT-CS Home Cover

XRD – X-ray Diffraction

Description:

X-ray Diffraction (XRD) is a powerful analytical technique used to investigate the structure of crystalline materials by analyzing the way X-rays are scattered by the crystal lattice. XRD is based on the principle of Bragg’s law, which states that X-rays incident on a crystal at a specific angle will undergo constructive interference and produce a diffraction pattern, which can be used to determine the crystal’s atomic arrangement.

Applications of X-ray Diffraction:

  1. Material Characterization: XRD is widely used to determine the crystal structure of materials. This includes the identification of phases in a sample, the lattice parameters, and the arrangement of atoms within the crystal lattice.
  2. Mineralogy and Geology: Geologists use XRD to analyze minerals and rocks, helping to identify and understand geological formations and mineral compositions.
  3. Pharmaceuticals: In the pharmaceutical industry, XRD is used to confirm the crystalline nature of drug compounds and to study their polymorphism, which can affect drug stability and bioavailability.
  4. Metallurgy: XRD is used to analyze the crystallography of metals and alloys, aiding in materials testing and quality control.
  5. Nanomaterials and Nanotechnology: Researchers use XRD to investigate the structure and properties of nanomaterials, which often exhibit unique properties due to their small size.
  6. Biology and Protein Crystallography: XRD plays a crucial role in determining the three-dimensional structures of biological macromolecules such as proteins and DNA.

Strengths of X-ray Diffraction:

  1. High Resolution: XRD can provide atomic-level structural information, making it one of the most powerful techniques for characterizing crystalline materials.
  2. Non-Destructive: XRD is non-destructive, meaning it does not damage the sample, making it suitable for studying valuable or irreplaceable materials.
  3. Wide Applicability: It can be applied to a wide range of materials, from small organic compounds to complex biological molecules and inorganic solids.
  4. Quantitative Analysis: XRD can provide quantitative information about phase composition, crystallite size, and other parameters.

Limitations of X-ray Diffraction:

  1. Requires Crystalline Materials: XRD is primarily applicable to crystalline materials. Amorphous or non-crystalline substances do not produce diffraction patterns.
  2. Sample Size and Preparation: Proper sample preparation is critical, and the sample size must be large enough to provide sufficient X-ray scattering.
  3. Complex Data Interpretation: Interpreting XRD data can be challenging, especially for complex crystal structures. Specialized software and expertise are often required.
  4. Instrumentation: High-quality XRD instruments can be expensive, limiting access for some laboratories.
  5. Radiation Exposure: XRD uses X-rays, which can be hazardous if not properly shielded and handled. Safety precautions must be followed.

In summary, X-ray Diffraction is a versatile and powerful technique for determining the crystal structure of a wide range of materials. Its non-destructive nature, high resolution, and quantitative capabilities make it a valuable tool in materials science, chemistry, geology, and various other fields, but it is limited to crystalline materials and requires expertise for accurate data interpretation.

Related Test Methods

EPR – Electron Paramagnetic Resonance

Goniometric Testing

UV-VIS

Scatterometry

xyy Color

Lab* Color

Reflectance

Transmission

Absorption

Emissivity

Deformulation

Rheology

Previous Post:MAT-CS Home CoverVPD-ICPMS – Vapor Phase Decomposition/ICPMS
Next Post:XRF – X-Ray FluorescenceMAT-CS Home Cover

Ready to start your analysis?

Get a Quote!
MAT-CS

Your One Source for Materials Analysis

1-800-685-2088

support@mat-cs.com

  • Home
  • Analytical Techniques
  • Test Methods
  • Resources
  • Contact Us
  • Get a Quote!
  • Special Analysis Request

  • LinkedIn

Copyright © 2025 by Materials Characterization Services · All Rights Reserved
Website Built, Hosted, and Managed by Digital Donkey Marketing